Caltech Micromachining Laboratory Electrolysis-Based On-Chip Dispensing System for ESI-MS

Project Abstract

We report here an integrated on-chip sample dispensing system for Electrospray Ionization-Mass Spectrometry (ESI-MS) applications. The stand-alone chip includes an electrolysis-based micropump, a passive micro mixer and an ESI nozzle. Operation of the chip doesn’t require any external fluidic coupling because the chip is designed to have samples filled, sealed and stored in reservoirs inside the chip before testing. Demonstrated here is a chip with two sample reservoirs and dispensing of the samples is electrically controlled individually. Experimentally, on-chip co-dispensing of two different samples is successfully achieved with a dispensing flow rate about 50 nl/min and a continuous spray for 2 minutes.

References

J. Xie, Q. He, Y.C. Tai, J. Liu and T. Lee, "Electrolysis-Based On-Chip Dispensing System for ESI/MS," Proceedings, The Sixteenth IEEE International Conference on Micro Electro Mechanical Systems (MEMS '03), Kyoto, Japan, Jan. 19-23, pp. 443-446, (2003).

Involved Personnel

Jun Xie, Qing He , Yu-Chong Tai, Jun Liu and Terry Lee

Related Publications

  • X.Q. Wang, A. Desai, Y.-C. Tai, L. Licklider, T.D. Lee, “Polymer-Based Electrospray Chips for Mass Spectrometry”, The 12th IEEE International Conference on Micro Electro Mechanical Systems (MEMS’99), Orlando, Florida, 1999, pp. 523-528

  • J. Xie, X. Yang, X.Q. Wang and Y.C. Tai, “Surface Micromachined Leakage Proof Parylene Check Valve”, The 14th IEEE International Conference on Micro Electro Mechanical Systems (MEMS’01), Interlaken, Switzerland, 2001, pp.539-542